Publication:
Electrochemical Determination of Uric Acid in Urine by Using Zeolite Imidazolate Framework-11 Modified Electrode

datacite.subject.fos oecd::Natural sciences
dc.contributor.author Tran Si Thanh
dc.contributor.author Phan Tu Qui
dc.contributor.author Nguyen Thi Thanh Tu
dc.contributor.author Tran Thanh Tam Toan
dc.contributor.author Tran Thi Bich Hoa
dc.contributor.author Le Van Thanh Son
dc.contributor.author Do Mai Nguyen
dc.contributor.author Tran Ngoc Tuyen
dc.contributor.author Dinh Quang Khieu
dc.contributor.editor Thanh-Danh Nguyen
dc.date.accessioned 2022-11-02T02:21:12Z
dc.date.available 2022-11-02T02:21:12Z
dc.date.issued 2021
dc.description.abstract In the present article, the synthesis of zeolite imidazole framework-11 (ZIF-11) by ultrasonic-assisted hydrothermal process and its application as an electrode modifier for electrochemical determination of uric acid in urine are demonstrated. The obtained materials were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), and nitrogen adsorption/desorption isotherms. It was found that the ZIF-11 with rhombic dodecahedron topology and high surface area (1066m2.g-1) was synthesized in a certain temperature and found in around 25–40°C, and other crystalline phases of zinc benzimidazolate deferring from ZIF-11 phase were found in less 25°C or higher than 40 ° C. The ZIF-11 is stable in the pH range 6-10. The modification of glassy carbon electrode was performed with ZIF-67 using the drop-casting procedure. The present ZIF-11 modified electrode was employed to study the electrochemical behavior of uric acid (UA). UA oxidation is catalyzed by this electrode in aqueous buffer solution (pH7) with a decrease of 70mV in overpotential compared to glassy carbon electrode. With the differential pulse–anodic stripping voltammetry (DP-ASV) method, the oxidation current of UA versus its concentration shows good linearity in the range 20– 540μM (R = 0:998) with a detection limit of 0.48 μM (S/N = 3). The obtained ZIF-11 modified electrode was applied in the detection of UA content in urine samples, and satisfied results were obtained.
dc.identifier.doi 10.1155/2021/9914062
dc.identifier.uri http://repository.vlu.edu.vn:443/handle/123456789/619
dc.language.iso en_US
dc.relation.ispartof Journal of Nanomaterials
dc.relation.issn 1687-4129
dc.relation.issn 1687-4110
dc.title Electrochemical Determination of Uric Acid in Urine by Using Zeolite Imidazolate Framework-11 Modified Electrode
dc.type journal-article
dspace.entity.type Publication
oaire.citation.volume 2021
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